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J. Korean Ceram. Soc. > Volume 52(1); 2015 > Article
Journal of the Korean Ceramic Society 2015;52(1): 56.
doi: https://doi.org/10.4191/kcers.2015.52.1.56
졸-겔법을 이용한 Al2O3가 분산된 TZP 단섬유의 제조
심수만
홍익대학교 재료공학부
Fabrication of Discontinuous Al2O3-Dispersed TZP Fibers by a Sol-Gel Method
Soo-Man Sim
School of Materials Science and Engineering, Hongik University
ABSTRACT
Discontinuous, polycrystalline $Al_2O_3$-dispersed TZP fibers were prepared by the centrifugal spinning of a colloidal $ZrO_2$ sol containing Y and Al nitrates and poly(vinyl alcohol). Factors affecting the rheological properties of the sols, such as sol concentrations, aging, and the amounts and types of additives, were investigated by measuring the shear viscosities. The flow characteristics of the sols were studied in relation to the spinnability by measuring the viscosity with respect to the shear rate. The spinnability was obtained through the addition of a polymer which increases the viscosity to a range of optimum viscosity values for spinning. Aging the sols containing the additives did not noticeably change the sol viscosities at room temperature up to 30 days. The flow behavior of the spinnable sols progressively changed from nearly Newtonian to pseudoplastic with an increase in the sol concentration.
Key words: Sol-gel method, Fiber, $Al_2O_3$-disperse TZP, Viscosity, Spinnability
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