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J. Korean Ceram. Soc. > Volume 48(2); 2011 > Article
Journal of the Korean Ceramic Society 2011;48(2): 178.
doi: https://doi.org/10.4191/kcers.2011.48.2.178
Rutile계 안료의 합성에 관한 연구
어혜진, 이병하
명지대학교 신소재공학과
A Study on the Synthesis of Rutile - Type Ceramic Pigments
Hye-Jin Eo, Byung-Ha Lee
Department of Material Science & Engineering, Myongji University
ABSTRACT
The Rutile - type brown pigments doped with chromium were synthesized. Samples of $Ti_{1-x}Cr_xO_2$ ($0.02{leq}X{leq}0.08$) were synthesized by the solid state method. Solid solution limit of Cr contents to the rutile structure and its coloration were studied. Optimum composition was investigated accordingly. The characteristics of synthesized pigments were analyzed by XRD, SEM, Raman spectroscopy and UV. As a result, single phase of Rutile was observed from $1000^{circ}C$ by XRD. The maximum limit of solid solution was 0.06 mole $Cr_2O_3$. The glazed sample showed brown color, and the value of CIE $L^*a^*b^*$ was $L^*$ 33.27, $a^*$ 10.64, $b^*$ 20.84.
Key words: Rutile, Anatase, Ceramic pigments, Brown
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