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J. Korean Ceram. Soc. > Volume 46(6); 2009 > Article
Journal of the Korean Ceramic Society 2009;46(6): 639.
doi: https://doi.org/10.4191/kcers.2009.46.6.639
SnO2-TiO2-V2O5계의 노랑안료 합성
주인돈, 황동하, 이현수, 박주석1, 이병하
명지대학교 공과대학 신소재공학과
1한국세라믹기술원 기업협력센터
Synthesis of SnO2-TiO2-V2O5 System Yellow Pigment
In-Don Joo, Dong-Ha Hwang, Hyun-Soo Lee, Joo-Seok Park1, Byung-Ha Lee
Department of Materials Science & Engineering, Myongji University
1Korea Institute of Ceramic Engineering and Technology
ABSTRACT
The research was performed to find out the optimum firing condition for the $SnO_2-TiO_2-V_2O_5$ system yellow pigment. The pigment based on $SnO_2-V_2O_5$ system showed very intense yellow color and it was used widely in ceramics industry. Synthesized pigment, with partial substitutions of $SnO_2;by;TiO_2$, was fired at $1300{^{circ}C}$ soaking 1h and it showed bright yellow color. $SnO_2-TiO_2-V_2O_5$ system was very more intensive changes in yellow color by colorimetric value $b^*$ than $SnO_2-V_2O_5$ system. Synthesized yellow pigments were characterized by X-ray diffraction (XRD), FT-IR, and UV-vis spectroscopy. The best composition for yellow pigment was 93:7:0.5(mole%) for $SnO_2-V_2O_5-TiO_2$. The measurement of CIE $L^*a^*b^*$ of pigment was $L^*(78.82),;a^*(-4.88);and;b^*$(59.25).
Key words: Yellow, Inorganic pigments, Cassiterite, $V_2O_5$, $TiO_2$
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