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J. Korean Ceram. Soc. > Volume 32(5); 1995 > Article
Journal of the Korean Ceramic Society 1995;32(5): 626.
자기파를 함유한 SiCwlf 세라믹스의 미세구조 제어
이성희
홍익대학교 무기재료공학과
The Microstructure Control of SiC Ceramics Containing Porcelain Scherben
ABSTRACT
The SiC-porcelain powder mixtures containing 51.9wt% SiC are produced as by-products from the surface abrasion process of porcelain cores. This raw powders were used as starting materials for the synthesis of SiC containing ceramics. The specimen, which was fired at 135$0^{circ}C$ from raw powders, had SiC, $Al_{2}O_{3}$, , cristobalite, mullite as crystalline phases, and the fractured microstructure showed dispersed SiC crystalline particles almost wetted with glassy matrix and spherical pores. Although the oxidation of SiC containing powder compacts wetted with glassy matrix and spherical pores. Although the oxidation of SiC containing powder compacts started at the range of 600~80$0^{circ}C$ form the analysis of weight gain, the presence of $SiO_{2}$ crystallien phase and cristobalite was confirmed at 100$0^{circ}C$ by XRD analysis. Mullitization of specimens was accelerated by preheating before the final firing. The specimen sintered at 135$0^{circ}C$ after 100$0^{circ}C$ preheating consisted of SiC, cristobalite, mullite as crystalline phases, and revealed 2.24g/$cm^{3}$ bulk density, 11.73% water adsorption, porous microstructure with small amount of glassy phase. SiC contents of specimens, which was 51.9 wt% in the raw powders, reduced to 37~22 wt% after firing at 135$0^{circ}C$ depending on the preheating condition.
Key words: SiC containing ceramics, By-product, Weight gain, Oxidation, SiC, $Al_{2}O_{3}$ mullite, Microstructure
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