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Journal of the Korean Ceramic Society 1987;24(2): 147. |
김천규석으로부터 질화규소의 합성 |
이홍림, 서원선, 조덕호1, 이종민1 |
연세대학교 공과대학 요업공학과 1국립공업시험원 |
Synthesis of Silicon Nitride from Kimcheon Quartzite |
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ABSTRACT |
ders were prepared by the simultaneous reduction and nitridation from powder mixtures of Kim cheon quartzite and carbon (graphite or carbon black) at1400$^{circ}C$ for 10 hours in nitrogen atmosphere. The effects of the reaction variables on the yield of products and on the ${alpha}$/${beta}$ ratio were examined. The average particle size, density, and the ${alpha}$/${beta}$ ratio of the obtained si3N4 were 1.0$mutextrm{m}$, 3.10g/㎤ and 90/10, respectively. It was found that the Si3N4 powders obtained in this work were comparable to the foreign commercial products. |
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