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Journal of the Korean Ceramic Society 1985;22(1): 40. |
하소온도가 PZT의 소결특성에 미치는 영향 |
정수태, 이우일1, 조상희1 |
부산개방대학 전자공학과 1경북대학교 전자공학과 |
Effect of Calcining Temperature on Sintering Characteristics of PZT |
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ABSTRACT |
The effect of calcining temperature ranged from $700^{circ}C$ to 110$0^{circ}C$ on sintering characteristics of morphotropic $Pb(Zr_{0.53}Ti_{0.47})O_3 doped with $Nb_2O_5$ has been investigated. The ratio of sintered grain size to calcined grain size decreased as the calcining temperature increased. The hardness as well as the sintered density of the samples reached a maximum at about 90$0^{circ}C$. The X-ray diffraction pattern of the sintered sample showed both tetragonal and rhombohedral phases. The tetragonal phases intensity increased with the calcining temperature going through a maximum at about 90$0^{circ}C$ while the rhombohedral phase intensity remained uneffected. The both intensity were about the same at 90$0^{circ}C$ The dielectric constant of the sintered samples reached a maximum um while the dielectric dissipation factor showed a minimum at the calcining temperature of about 100$0^{circ}C$ |
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