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J. Korean Ceram. Soc. > Volume 42(11); 2005 > Article
Journal of the Korean Ceramic Society 2005;42(11): 743.
doi: https://doi.org/10.4191/kcers.2005.42.11.743
수열합성법으로 제조된 PZT 분말의 특성에 미치는 광화제 농도와 출발물질의 영향
양범석, 윤기석1, 박영철2, 원창환
충남대학교 급속응고신소재연구소
1한국에너지기술연구원
2(주)씨에라 인더스트리
Effect of Mineralizer Concentration and Starting Materials on the Characteristics of PZT Powders by Hydrothermal Process
Beom-Seok Yang, Ki-Seok Yun1, Young-Chul Park2, Chang-Whan Won
Engineering Research Center for Rapidly Solidified Materials, Chungnam National University
1Korea Institute of Energy Research
2Sierra Industry Co. LTD.
ABSTRACT
The effect of reaction parameters in the characteristic of $Pb(Zr_{0.52} Ti_{0.48})O_3$ powders by hydrothermal process was investigated in this study. In the preparation of PZT, the types of starting material and concentration of mineralizer on phase fraction and morphology was investigated respectively. Regardless the types of Pb precursor, PZT was able to synthesize ranging from 7 to 20 on KOH concentration and from 13.01 to 13.55 on pH of solution. The particle size of the PZT powders can be controlled by the mineralizer concentration and various types of precursor.
Key words: Hydrothermal process, Particle size, Mineralizer, Phase fraction
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