석탄계 피치에 요오드를 소량 첨가하여 제조한 탄소복합재의 치밀화 거동 |
조광연, 류도형, 신동근, 주혁종1, 구형회2, 박인서2 |
한국세라믹기술원 미래융합세라믹본부 1충남대학교 고분자공학부 2국방과학연구소 제4기술연구본부 |
Densification Behavior of C/C Composite Derived from Coal Tar Pitch with Small Amount of Iodine Addition |
Kwang-Youn Cho, Doh-Hyung Riu, Dong-Geun Shin, Heyok-Jong Joo1, Hyung-Hoi Koo2, In-Seo Park2 |
Division of Nano Materials Application, KICET 1Department of Polymer Science and Engineering, Chungnam University 2Agency for Defense Development |
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ABSTRACT |
We investigated the viscosity behavior and the carbon yield of coal tar pitch (CTP) treated with iodine. The viscosity of iodine treated pitch showed that the fluidity of iodine treated CTP did not increase within the iodine addition of 1.4%. DTG analysis showed that cross linking was accelerated at the temperature range from $400;to;500{^{circ}C}$ with iodine treatment, which is due to the accelerated dehydrogenative reaction by iodine. The iodine treatment was mainly effective for β-resin content increase of CTP. The carbon yield of CTP increased from 40 to 60% by the iodine non-treated CTP. |
Key words:
C/C composite, Viscosity, Carbon yield, Iodine, Pitch |
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