방전플라즈마 소결법에 의한 탄화 붕소 세라믹스의 소결 거동 및 기계적 특성 |
김경훈, 채재홍, 박주석, 김대근, 심광보1, 이병하2 |
요업기술원 1한양대학교 신소재공학부 2명지대학교 신소재공학부 |
Sintering Behavior and Mechanical Property of B4C Ceramics Fabricated by Spark Plasma Sintering |
Kyoung-Hun Kim, Jae-Hong Chae, Joo-Seok Park, Dae-Keun Kim, Kwang-Bo Shim1, Byung-Ha Lee2 |
Korea Institute of Ceramic Engineering and Technology 1Division of Advanced Materials Science and Engineering, Hanyang University 2Department of Materials Science and Engineering, Myongji University |
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ABSTRACT |
[ $B_4C$ ] ceramics were fabricated by spark plasma sintering process and their sintering behavior, microstructure and mechanical properties were evaluated. Relative density of $B_4C$ ceramics could be achieved by spark plasma sintering method reached as high as 99% at lower temperature than conventional sintering method, in addition, without any sintering additives. The mechanical properties of $B_4C$ ceramics could be improved by the heat treatment at $1300^{circ}C$ during sintering process which can be removed $B_2O_3$ phase from a $B_4C$ powder surface. This improvement results from the formation of a fine and homogeneous microstructure because the grain coarsening was suppressed by the elimination of $B_2O_3$ phase. Particularly, mechanical properties of the specimen experienced the $B_2O_3$ removing process improved over 30% compared with the specimen without that process. |
Key words:
$B_4C$, Microstructure, Mechanical property, Spark plasma sintering |
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