Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN Composite

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J. Korean Ceram. Soc. > Volume 33(7); 1996 > Article

Journal of the Korean Ceramic Society 1996;33(7): 785.

상압소결에 의하여 제조된 SiC-AlN 복합체에서의 고용체 형성과 미세구조

이종국, 김덕준¹, 김환¹

조선대학교 재료공학과
¹서울대학교 무기재료공학과

Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN Composite

ABSTRACT

Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN compo-site using oxides as a sintering aid at 185$0^{circ}C$ and 195$0^{circ}C$ Regardless of SiC/AlN ratio in composition most of sintered specimens showed he complex structure mixed with 2H solid solution and SiC particles. High sintering temperature and large AlN content in starting composition enhanced the formation of 2H solid solution in sintered specimen 2H solid solution showed the spherical shape and core-rim structure. AlN content in the core is higher than that in the rim but SiC content . The size of 2H solid solution on fracture showed the transgranular fracture mode compared with the dispersed SiC particles which showed the intergranular fracture mode.

Key words: SiC-AlN composites, Microstructure, Pressureless sintering, 2H solid solution